4.6 Article

Consecutive reactions between methyl 3-dehydroshikimiate, amines and 1,2-dichloroalkanes under microwave conditions: a practical, one-pot construction of N-substituted dihydrobenzoxazines

Journal

RSC ADVANCES
Volume 4, Issue 20, Pages 10022-10027

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra47221c

Keywords

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Funding

  1. National Science Foundation of China [21272280, 81201716, 81301890]
  2. Science & Technology Program of Guangdong Province [S2013010014278, 2011A081401002, 2012B091100241]
  3. Zhejiang Province [LY1 3H160010, 2012ZQ017]
  4. Guangzhou City [2012J4300097]

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A biomass-involved, one-pot, two-step protocol for the synthesis of N-substituted 3,4-dihydro-2H-1,4-benzoxazines has been developed. A wide range of new compounds have been efficiently synthesized in moderate to excellent yields via the three-component consecutive reactions between methyl 3-dehydroshikimiate (3-MDHS), amines and 1,2-dichloroalkanes in short reaction times under microwave conditions.

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