Journal
RSC ADVANCES
Volume 4, Issue 20, Pages 10022-10027Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra47221c
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Funding
- National Science Foundation of China [21272280, 81201716, 81301890]
- Science & Technology Program of Guangdong Province [S2013010014278, 2011A081401002, 2012B091100241]
- Zhejiang Province [LY1 3H160010, 2012ZQ017]
- Guangzhou City [2012J4300097]
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A biomass-involved, one-pot, two-step protocol for the synthesis of N-substituted 3,4-dihydro-2H-1,4-benzoxazines has been developed. A wide range of new compounds have been efficiently synthesized in moderate to excellent yields via the three-component consecutive reactions between methyl 3-dehydroshikimiate (3-MDHS), amines and 1,2-dichloroalkanes in short reaction times under microwave conditions.
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