Journal
RSC ADVANCES
Volume 4, Issue 20, Pages 10001-10012Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra47466f
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Funding
- Council of Scientific and Industrial Research (CSIR)
- Department of Science and Technology (DST), New Delhi, India
- DST, India
- University Grant Commission (UGC)
- CSIR-India
- DST
- UGC, New Delhi
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A graphene based composite with silver nanoparticles has been synthesized via a simple chemical route and its catalytic activity has been tested for multi-component reactions and click reaction in a one-pot approach. This silver-graphene nanocomposite shows excellent catalytic activity at room temperature for three-component couplings between aldehydes, alkynes and amines (A(3)-coupling) and one-pot synthesis of 1,4-disubstituted 1,2,3-triazole via click reaction between in situ generated azides (derived from anilines or amines) and terminal acetylenes. This solid silver-graphene catalyst has been characterized by TEM, Raman, XRD and UV-Visible absorption spectra. The developed catalyst is air-stable, inexpensive, easy to prepare and can be facilely recovered and reused five times without significant decrease in activity and selectivity.
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