Journal
RSC ADVANCES
Volume 4, Issue 35, Pages 17969-17979Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ra01736f
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Funding
- Council of Scientific and Industrial Research, New Delhi
- CSIR for research fellowships
- Department of Science and Technology for providing HRMS facility in DST-FIST program
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A highly efficient and rapid method for the synthesis of 2-hydroxy-1,4-benzoxazine and butenolide derivatives has been developed. The key step in this protocol involves the reduction of benzoxazinone derivatives. Further reaction of 2-hydroxy-1,4-benzoxazine with secondary amines and sodium methoxide affords the corresponding 2-amino-1,4-benzoxazines and butenolide derivatives, respectively, in good yields.
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