Journal
RSC ADVANCES
Volume 4, Issue 16, Pages 8278-8282Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra46745g
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Funding
- Engineering and Physical Sciences Research Council [EP/I007989/1]
- Engineering and Physical Sciences Research Council [EP/I007989/1] Funding Source: researchfish
- EPSRC [EP/I007989/1] Funding Source: UKRI
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We investigate the utility of pure shift techniques in revealing heteronuclear couplings in complex H-1 NMR spectra. The results show the technique to be a robust and valuable complement to the standard H-1 spectrum, and an attractive alternative to heteronuclear decoupling since the technique is independent of the size of the heteronuclear couplings and the chemical shift range(s) of the heteronuclei involved. We highlight some possible artefacts, and the subtle effects due to the presence of C-13 nuclei in otherwise symmetric molecules when bilinear rotational decoupling (BIRD) elements are present in the pulse sequence.
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