Journal
RSC ADVANCES
Volume 3, Issue 26, Pages 10158-10162Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra41262h
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A straightforward chromatography-free preparation of Weinreb amides starting from acid halides has been achieved in the biphasic medium 2-MeTHF/water. Analytically pure compounds were isolated in excellent yields simply after removal of 2-MeTHF, which absolutely avoids the use of any contaminant organic solvent within the whole process due to its (practically) immiscibility with water.
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