Journal
RSC ADVANCES
Volume 2, Issue 24, Pages 9179-9182Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ra21667a
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Funding
- Research Grants Council of Hong Kong [CERG: PolyU5012/09P]
- State Key Laboratory of Chirosciences [4-BBX3]
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This study reports the first general Pd-catalyzed direct arylation of polyfluoroarenes with aryl tosylates/mesylates. A wide range of polyfluoroarenes can be coupled with both aryl tosylates and mesylates under relatively mild reaction conditions (90 degrees C, in the presence of a weak base KOAc, without any additional acid additives). Moreover, a one-pot sequential C-H bond functionalization/C-N bond coupling has been successfully accomplished by employing one single Pd/CM-phos catalyst system.
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