Journal
GREEN CHEMISTRY LETTERS AND REVIEWS
Volume 5, Issue 3, Pages 329-336Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/17518253.2011.631942
Keywords
glycerol; disulfides; green chemistry; microwave
Funding
- FAPERGS [FAPERGS/PRONEX 10/0005-1, 10/0027-4]
- CAPES
- FINEP
- CNPq
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We present here a clean and fast synthesis of organic disulfides starting from thiols using glycerol as solvent under microwave irradiation. This efficient method is general for aromatic, aliphatic, and functionalized thiols, affording the corresponding disulfides in good to excellent yields after easy work up. Glycerol can be easily recovered and utilized for further oxidation reactions.
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