4.1 Article

Synthesis and Crystal Growth of Tetragonal β-Fe1.00Se

Journal

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
Volume 640, Issue 8-9, Pages 1600-1606

Publisher

WILEY-V C H VERLAG GMBH
DOI: 10.1002/zaac.201300670

Keywords

Chemical vapor transport; Superconductivity; Selenium; Iron

Funding

  1. DFG [SPP 1458]

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Single crystals of tetragonal beta-Fe1.00Se were grown from polycrystalline material by chemical vapor transport reaction at temperatures below 723 K using AlCl3 as transport additive. The plate-shaped single crystals have edge lengths up to 4 mm. The single crystals display complete diamagnetic shielding 4 pi chi approximate to -1 below the super-conducting transition.

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