Journal
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
Volume 637, Issue 12, Pages 1693-1701Publisher
WILEY-BLACKWELL
DOI: 10.1002/zaac.201100263
Keywords
Alkaline earth metals; Tetrazoles; Crystal structures; IR spectroscopy; Pyrotechnics
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Funding
- Ludwig Maximilian University of Munich (LMU)
- U.S. Army Research Laboratory (ARL)
- Armament Research, Development and Engineering Center (ARDEC)
- Strategic Environmental Research and Development Program (SERDP)
- Office of Naval Research (ONR Global) [W911NF-09-2-0018, W911NF-09-1-0120, W011NF-09-1-0056, 10 WPSEED01-002 / WP-1765]
- The Cusanuswerk
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The alkaline earth metal salts of 5,5 '-BT, [Be(H(2)O)(4)](5,5 '-BT)center dot H(2)O (1), [Mg(H(2)O)(6)(5,5 '-BT)center dot 3H(2)O (2), [Ca(H(2)O)(4)(5,5 '-BT)]center dot H(2)O (3), [Sr(H(2)O)(4)(5,5 '-BT)]center dot 2DMF (4), and [Ba(H(2)O)(4)(5,5 '-BT)] (5) were fully characterized by low temperature X-ray diffraction, vibrational (IR, Raman) and NMR spectroscopy, elemental analysis and differential scanning calorimetry (DSC). A detailed description of the crystal structures is given. In addition, the potential use of 4 and 5 in coloring pyrotechnical compositions was investigated.
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