Journal
ULTRASONICS SONOCHEMISTRY
Volume 50, Issue -, Pages 1-5Publisher
ELSEVIER
DOI: 10.1016/j.ultsonch.2018.08.001
Keywords
C-H activation; Ultrasound-assisted; Cu-catalyzed; Benzo[1,3]thiazine; Isocyanides; Aniline; Isothiocyanate
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Funding
- National Institute for Medical Research Development (NIMAD) [962440]
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A facile sonochemical route for the synthesis of benzo[1,3]thiazine derivatives via a one pot, multicomponent, intramolecular C-H activation reaction from isocyanides, aniline and benzoyl (acetyl) isothiocyanate adduct catalyzed by copper (I) iodide in acetone at 30 degrees C have been reported. The advantages of the described method include using simple and readily available starting materials and performing under mild copper-catalytic reaction conditions and also obtaining pure product with high yield without applying column chromatography. Furthermore, using the sonochemical methodology as an efficient method led to reduce the reaction times.
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