4.7 Article

Environmentally friendly sonocatalysis promoted preparation of 1-thiocarbamoyl-3,5-diaryl-4,5-dihydro-1H-pyrazoles

Journal

ULTRASONICS SONOCHEMISTRY
Volume 16, Issue 6, Pages 728-731

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.ultsonch.2009.02.005

Keywords

Ultrasound irradiation; Pyrazoles; Sonocatalysis; Green chemistry

Funding

  1. FAPESP [06/58124-3, 06/56315-6]
  2. CEPEMA-USP (Centro de Capacitacao e Pesquisa ern Meio Ambiente)
  3. CNPq [310472/2007-5]
  4. CAPES

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An efficient and green synthesis of thiocarbamoyl-3,5-diaryl-4,5-dihydro-1 H-pyrazoles via the condensation of chalcones with thiosemicarbazide in ethanol and KOH under ultrasound irradiation is reported. The products were isolated in good yields after short reaction times. (C) 2009 Elsevier B.V. All rights reserved.

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