Journal
ACS SUSTAINABLE CHEMISTRY & ENGINEERING
Volume 3, Issue 9, Pages 2058-2066Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acssuschemeng.5b00325
Keywords
Bis-lawsones; Functionalized 3,3 '-(aryl/alkyl-methylene)bis(2-hydroxynaphthalene-1,4-dione) scaffolds; Sulfamic acid; Aqueous ethanol; Room-temperature; No column chromatography; Green and sustainable chemistry
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Funding
- Council of Scientific and Industrial Research, New Delhi [02(0110)112/EMR-II]
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A simple and energy-efficient green protocol for the synthesis of a series of biologically interesting functionalized bis-lawsone [i.e., 3,3'-(aryl/alkyl-methylene)bis(2-hydroxynaphthalene-1,4-dione)] scaffolds has been developed in the presence of sulfamic acid as an eco-friendly organocatalyst via one-pot pseudomulticomponent reaction at room temperature. The salient features of the present protocol are mild reaction conditions, good to excellent yields, operational simplicity, energy-efficiency, high atom-economy, eco-friendliness, easy isolation of products and no column chromatographic separation.
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