Journal
TRANSITION METAL CHEMISTRY
Volume 39, Issue 1, Pages 33-39Publisher
SPRINGER
DOI: 10.1007/s11243-013-9769-6
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- University of Zanjan
- Ministry of Science, Research and Technology of the I.R. Iran [213631]
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A new mononuclear complex of vanadium(V), [V(O)(bp)(OCH3)] (1) has been synthesized, where H(2)bp is N,N'-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-N',N'-dimethylethylene-1,2-diamine. The complex was characterized by elemental analyses, spectroscopic methods and X-ray diffraction measurement. Single-crystal X-ray diffraction structure analysis of the complex revealed that the vanadium atom is octahedrally coordinated and that the bis(phenolate) ligand (bp(2-)) is N2O2-bonded to the vanadium(V) center in a tetradentate dinegative fashion.
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