Journal
TRANSITION METAL CHEMISTRY
Volume 34, Issue 5, Pages 549-557Publisher
SPRINGER
DOI: 10.1007/s11243-009-9228-6
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Funding
- CSIR, New Delhi [[01 (1818)/02/EMR-II]]
- DST, Govt. of India
- EPSRC
- University of Reading
- UGC, New Delhi [SR/SI/IC/12/2002]
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[MoO(O-2)(2)(PyCOXH)(H2O)] and PMePh3[MoO(O-2)(2)(PyCO)] (PyCOXH = Pyridine-2-carboxaldoxime and PyCOH = Pyridine-2-carboxylic acid) have been synthesized. Both complexes have been characterized by physico-chemical and spectroscopic methods; in addition, the carboxylate complex has been structurally characterized by X-ray crystallography. The carboxylate complex is a more efficient catalyst than the oxime complex for epoxidation of olefins and shows excellent catalytic activity for the substrates: cyclooctene, cinnamyl alcohol, allyl alcohol and 1-hexene.
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