Journal
THERMOCHIMICA ACTA
Volume 528, Issue -, Pages 85-89Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.tca.2011.11.003
Keywords
Bi(III) complexes; Thermal decomposition; X-ray diffraction; DTA; TG-MS; DSC
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An investigation of the interaction of Bi(III) with an aqueous solution of sulfanilic acid at a higher temperature is performed. As a result, a new composition [Bi6O6(OH)(2)](NH2C6H4SO3)(4) is precipitated. This Bi(III) complex is characterized by various methods: elemental analysis, DTA, TG- MS, DSC, FTIR, and powder X-ray diffraction. Based on the experimental results, X-ray diffraction indexation as well as thermal decomposition products of the compound are suggested. (C) 2011 Elsevier B.V. All rights reserved.
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