Journal
TETRAHEDRON-ASYMMETRY
Volume 19, Issue 13, Pages 1600-1607Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2008.06.015
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Racemic as well as enantiomerically pure trans-1,1'-(cyclohexane-1,2-diyl)bis(imidazole N-oxides) were prepared from trans-cyclohexane-1,2-bis(methylidenamine) and 1,2-dione monooximes (alpha-hydroxyiminoketones). The enantiomeric purity of selected products was determined by means of H-1 NMR spectroscopy in the presence of (+)-(R)-(tert-butyl)(phenyl)phosphonothioic acid as a chiral solvating agent. Deoxygenation by treatment with Raney-nickel led to the corresponding chiral bis-imidazoles. (C) 2008 Elsevier Ltd. All rights reserved.
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