Journal
TETRAHEDRON LETTERS
Volume 55, Issue 45, Pages 6193-6197Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2014.09.057
Keywords
Porphyrinoids; Acetoxylation; Crystal structure; H-1 NMR spectroscopy; UV-vis spectroscopy
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Funding
- MEXT [25105537, 24108730, 21245016, 25288031, NPS13103]
- Tokuyama Science Foundation
- Grants-in-Aid for Scientific Research [21245016, 24108730, 25288031, 25105744] Funding Source: KAKEN
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A series of multiply meso-substituted porphycenes has been prepared by acetoxylation of 2,7,12,17-tetra-n-propylporphycene (H2TPrPc), and the molecular structure of 9,10-diacetoxy-2,7,12,17-tetra-n-propylporphycene (2a) determined by single-crystal X-ray diffraction analysis. The H-1 NMR and optical properties have also been investigated. (C) 2014 Elsevier Ltd. All rights reserved.
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