Journal
TETRAHEDRON LETTERS
Volume 55, Issue 30, Pages 4102-4104Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2014.05.098
Keywords
Cyclopropylhydrazine; Copper salt-catalyzed addition; Cyclopropylboronic acid; Azodicarboxylate
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An efficient procedure for the synthesis of cyclopropylhydrazine in the form of its salts is reported. The copper salt-catalyzed addition of cyclopropylboronic acid to the azo group of di-tert-butyl azodicarboxylate and subsequent deprotection gave the cyclopropylhydrazine salts in high yields. (C) 2014 Elsevier Ltd. All rights reserved.
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