Journal
TETRAHEDRON LETTERS
Volume 55, Issue 34, Pages 4742-4746Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2014.06.086
Keywords
Alkenes; Sodium arenesulfinates; AgNO3/K2S2O8 catalysis; Aerobic oxysulfonylation; beta-Keto sulfones
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Funding
- CSIR [09/001(0379)/2013-EMR-I]
- DST [SR/S1/OC-22/2010]
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An efficient, AgNO3/K2S2O8 catalyzed one-pot radical route to beta-keto sulfones from alkenes is reported. The protocol involves oxysulfonylation of alkenes with air (O-2) and inexpensive sodium arenesulfinate salts under mild conditions. It is highly practical and allows the use of easily available starting materials in an open flask and aqueous medium at ambient temperature. (C) 2014 Elsevier Ltd. All rights reserved.
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