Journal
TETRAHEDRON LETTERS
Volume 55, Issue 10, Pages 1726-1728Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2014.01.102
Keywords
Bismuth nitrate as nitrite source; Catalyst free reaction; Potassium aryltrifluoroborates; Microwave
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Funding
- US department of education Title III Grant, Tennessee State University
- NIH's MARC (National Institutes of Health) [2T34GM007663-32]
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A mixture of bismuth nitrate pentahydrate and potassium aryltrifluoroborate in toluene under microwave heating at 120 degrees C for 20 min provides an interesting and mild reaction protocol for the synthesis of aryl nitrite. The conversion to aryl nitrites from aryltrifluoroborates without transition metal catalyst and base in high yields is remarkable. (c) 2014 Elsevier Ltd. All rights reserved.
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