Journal
TETRAHEDRON LETTERS
Volume 54, Issue 45, Pages 6101-6104Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2013.08.118
Keywords
Heck reaction; Cross-coupling; C-glycosides; Halo-exo-glycals; endo-Glycals
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Funding
- 'Zhu Xue' Talent Plan of Fudan University
- National Natural Science Foundation of China [21002014]
- Fundamental Research Funds for the Central Universities [10FX061]
- Scientific Research Foundation for the Returned Overseas Chinese Scholars [41th]
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An effective Heck-type cross-coupling reaction between halo-exo-glycals and endo-glycals to achieve C-glycosidic disaccharides has been developed. Using Pd(OAc)(2) as the catalyst, dppp as ligand and K2CO3 as base, the reactions gave C-glycosidic products in good to excellent yields with exclusive stereochemistry. (C) 2013 Elsevier Ltd. All rights reserved.
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