Journal
TETRAHEDRON LETTERS
Volume 54, Issue 10, Pages 1309-1311Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.12.101
Keywords
Vinyl halides; Iodotrimethylsilane; Haloenamides; Hydroiodation; Ynamides
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Funding
- Suzuken Memorial Foundation
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A facile approach to (E)-alpha-haloenamide moieties from ynamides using bromo- or iodotrimethylsilane is described. The simple protocol enables a regio- and stereospecific hydrohalogenation of the triple bond in gram-scale and provides a general entry for synthesis of novel enamide analogues. (C) 2012 Elsevier Ltd. All rights reserved.
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