Journal
TETRAHEDRON LETTERS
Volume 54, Issue 20, Pages 2538-2541Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2013.03.031
Keywords
Self-assembling organogels; Deuterated amines; Supramolecular chemistry; Solid state deuterium NMR
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Funding
- NCRIS
- Australian Research Council [DP09855059, FT120100101]
- Australian Research Council [FT120100101] Funding Source: Australian Research Council
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A general, direct and scalable synthesis of per-deuterated alkyl amines is reported, together with their incorporation into pyromellitamides, which form self-assembled gels in cyclohexane. The deuterium labelling of these gelators allows the study of the dynamic intermolecular interactions in these materials using solid-state H-2 NMR spectroscopy. Crown Copyright (C) 2013 Published by Elsevier Ltd. All rights reserved.
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