☆ 4.4 Article

A highly sensitive fluorescence method reveals the presence of palladium in a cross-coupling reaction mixture not treated with transition metals

TETRAHEDRON LETTERS (2012)

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Journal

TETRAHEDRON LETTERS
Volume 53, Issue 25, Pages 3147-3148

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.04.043

Keywords

Palladium; Suzuki-Miyaura coupling; Sensor; Fluorescence spectroscopy; Catalysis

Categories

Chemistry, Organic

Funding

  1. US National Science Foundation [CHE-0911092]
  2. Japan Society for the Promotion of Science [23790002]
  3. Direct For Mathematical & Physical Scien
  4. Division Of Chemistry [0911092] Funding Source: National Science Foundation
  5. Grants-in-Aid for Scientific Research [23790002] Funding Source: KAKEN

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We previously reported a Suzuki-Miyaura coupling in dimethyl carbonate without adding additional transition metals. Here, we show an analysis of the reaction mixture that revealed the presence of palladium using a fluorogenic Tsuji-Trost reaction. (C) 2012 Elsevier Ltd. All rights reserved.

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