Journal
TETRAHEDRON LETTERS
Volume 53, Issue 9, Pages 1180-1182Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.12.106
Keywords
Phenacenes; Borylation; Iridium; Regio-selectivity
Categories
Funding
- KAKENHI [21685005, 2010 8015, 22550094]
- NEDO
- JST
- Global COE Program (Molecular Complex Chemistry)
- Grants-in-Aid for Scientific Research [22550094, 21685005] Funding Source: KAKEN
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Iridium-catalyzed borylation of phenacenes with bis(pinacolato)diboron proceeds either in an edge-selective manner for diborylation or an edge/side-selective manner for tetraborylation. Multiply borylated [n]phenacenes (n = 3-5) were synthesized in reasonable yields. (C) 2011 Elsevier Ltd. All rights reserved.
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