Journal
TETRAHEDRON LETTERS
Volume 53, Issue 22, Pages 2694-2698Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.03.067
Keywords
Liebeskind-Srogl reaction; 2-Aryl-1,4-dihydropyrimidines; Dihydropyrimidinthiones; Tributyltin derivatives
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Funding
- Foundation of French-China Science and its Application (FFCSA)
- China Scholars Council (CSC)
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We developed an optimized Liebeskind-Srogl reaction in order to synthesize potentially biologically active 2-aryl-1,4-dihydropyrimidines. The pallado-catalyzed cross-coupling reaction between dihydropyrimidines and tributyltin derivatives appears particularly efficient (67-95% yields) when using CuBr.Me2S as the copper cofactor. (C) 2012 Elsevier Ltd. All rights reserved.
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