Journal
TETRAHEDRON LETTERS
Volume 53, Issue 42, Pages 5578-5581Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.07.143
Keywords
Photochemistry; Microflow; Terebic acid; Photoaddition
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Funding
- James Cook University [JCU-CRIG 2011]
- Global Initiatives Program
- Ministry of Education, Culture, Sports, Science and Technology of the Japanese Government
- Japan Student Service Organization (JASSO)
- Grants-in-Aid for Scientific Research [24106729] Funding Source: KAKEN
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The continuous-microflow photochemical synthesis of terebic acid from maleic acid was investigated in two different microreactor set-ups. The results were subsequently compared to analogue experiments in a conventional chamber reactor. Based on conversion rates, reactor design and energy efficiency calculations, the simple microcapillary reactor showed the best overall performance. (C) 2012 Elsevier Ltd. All rights reserved.
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