Journal
TETRAHEDRON LETTERS
Volume 53, Issue 24, Pages 2980-2984Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.03.086
Keywords
Nickel hydroxyapatite; Green chemistry; Henry reaction; Heterogeneous catalysis
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Funding
- Department of Science and Technology (DST), Ministry of science and Technology, Government of India, New Delhi [SR/S1/IC-45/2007]
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The utility of nickel hydroxyapatite nanocomposite (Ni-HAp) as a green catalyst for solvent free, microwave-assisted Henry reaction using nitromethane and a series of aromatic aldehydes as substrates is presented. The selected catalyst performed well to afford the respective nitrostyrenes which were quantified by gas chromatography equipped with a mass spectral detector (GC-MS). A few of the products were identified from the respective nuclear magnetic resonance (NMR) spectral data. (C) 2012 Elsevier Ltd. All rights reserved.
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