Journal
TETRAHEDRON LETTERS
Volume 52, Issue 11, Pages 1173-1175Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.01.018
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Funding
- Ministry of Education, Culture, Sports, Science and Technology, Japan
- Grants-in-Aid for Scientific Research [22550032] Funding Source: KAKEN
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The first total synthesis of (+)-batzellaside B and its C8-epimer was completed from a known L-arabinose-derived tribenzyl ether ill 22 steps with overall yields of 3.9% and 5.4%, respectively. The absolute configuration of (+)-batzellaside B was unambiguously determined to be 1S,3S,4S,5R,8S by the Mosher analysis of a synthetic intermediate prepared through a separate route. (C) 2011 Elsevier Ltd. All rights reserved.
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