Journal
TETRAHEDRON LETTERS
Volume 52, Issue 11, Pages 1176-1178Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.01.009
Keywords
Suzuki-Miyaura cross coupling; Solid-supported palladium; Heterogeneous catalyst; Nano and microparticles; Ligand free
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Funding
- Department of Science & Technology (Nano Mission), New Delhi [SR/NM/NS-95/2009]
- CSIR, New Delhi
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Solid-supported nano and microparticles of Pd(0) (SS-Pd) were prepared and used as heterogeneous catalysts for Suzuki-Miyaura cross coupling reactions of aryl halides (chloro, bromo and iodo) and phenyl boronic acid under mild and ligand-free conditions. Scanning electron microscope (SEM) and UV-vis based studies were performed to observe the distribution of nano and microparticles of palladium over solid surface and their oxidation states. In addition, the catalyst could be reused up to seven runs without significant loss of activity and stable enough under moist conditions. (C) 2011 Elsevier Ltd. All rights reserved.
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