Journal
TETRAHEDRON LETTERS
Volume 52, Issue 46, Pages 6098-6102Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.09.017
Keywords
alpha-Methylene-alpha-tetralones; Prins reaction; N-methylanilinium trifluoroacetate; Paraformaldehyde; Spirolactone
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Funding
- IIT Kanpur
- IIT Kharagpur
- CSIR, New Delhi
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alpha-Methylene-alpha-tetralone dimers (8-10) are shown to undergo a diastereoselective Prins reaction with paraformaldehyde in the presence of N-methylanilinium trifluoroacetate resulting in 2, 4, and 5. The structure of the new scaffold 2 was confirmed by X-ray crystallographic analysis. (C) 2011 Elsevier Ltd. All rights reserved.
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