Journal
TETRAHEDRON LETTERS
Volume 51, Issue 40, Pages 5265-5268Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2010.07.150
Keywords
Curtius rearrangement; Glycosidic linkage; Stereochemistry; Ring-opening reaction
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Funding
- Italian Ministero dell'Istruzione, dell'Universita e della Ricerca [MIUR 2005033023_001]
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A simple, convergent synthesis of the N-carbonyloxy beta-D-glucuronide of mexiletine (sodium salt) in moderate yield is described. The compound is now available as an authentic reference standard for analytical studies, enabling more detailed investigation on the metabolism of mexiletine. (C) 2010 Elsevier Ltd. All rights reserved.
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