Journal
TETRAHEDRON LETTERS
Volume 51, Issue 18, Pages 2473-2476Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2010.02.154
Keywords
Glycoluril clip; Immobilization; Merrifield resin; Dihydroxybenzenes; Affinity chromatography
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A practical method for the separation and purification of dihydroxybenzenes from phenol-dihydroxybenzene, methoxyphenol-dihydroxybenzene, and isomeric dihydroxybenzene mixtures was developed on the basis of affinity chromatography using a functionalized Merrifield resin. The resin was obtained by immobilization of a glycoluril-derived clip on Merrifield resin. This recyclable resin was repeatedly used for convenient and rapid separation of dihydroxybenzenes from the above-mentioned mixtures. (C) 2010 Elsevier Ltd. All rights reserved.
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