Journal
TETRAHEDRON LETTERS
Volume 51, Issue 15, Pages 2036-2038Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2010.02.046
Keywords
Transglycosylation; Artificial deoxyribonucleoside; Puckering conformation
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Funding
- KAKENHI [20655026/20108015]
- JSPS
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Deoxyribonucleoside analogues bearing acetylene group at the pseudo-5'-position and azido group at the pseudo-3'-position have been synthesized by transglycosylation reaction of deoxythymidine analogue with adenine, cytosine, and guanine nucleobases as nucleophiles. The structures of analogues were studied in crystalline state by X-ray crystallography as well as in solution phase by NMR spectroscopy and showed the puckering conformations similar to the natural congeners. (C) 2010 Elsevier Ltd. All rights reserved.
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