Journal
TETRAHEDRON LETTERS
Volume 50, Issue 52, Pages 7395-7398Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.10.090
Keywords
alpha,beta-Epoxyketoximes; gamma-Hydroxy-alpha-nitroolefins; Oxidation; Hypervalent iodine; IBX; DMP
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Funding
- Ministry of Science and Innovation of Spain [CTQ2008-04024, AGL2009-12266-C02-02]
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An efficient method for the preparation of gamma-hydroxy-alpha-nitroolefins from alpha,beta-epoxyketoximes has been developed using IBX. The reaction occurs at room temperature Without the formation of over-oxidation products and also has an easy work-up procedure. (C) 2009 Elsevier Ltd. All rights reserved.
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