Journal
TETRAHEDRON LETTERS
Volume 49, Issue 5, Pages 893-895Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.11.167
Keywords
iodination; halogenation; haloperoxidation; hydrogen peroxide; green chemistry; aerobic halogenation; organo-halogen compounds
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Aerobic oxidative iodination activated by sodium nitrite occurs effectively and selectively with 100% iodine atom economy with air as the oxidant. Silica-supported sulfuric acid was used for the activation of the catalyst and iodination. Thus, I(2)/NaNO(2)/air/silica-supported H(2)SO(4) in acetonitrile iodinated aromatics, ketones and aldehydes effectively at ambient temperature. (C) 2007 Elsevier Ltd. All rights reserved.
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