Journal
TETRAHEDRON LETTERS
Volume 49, Issue 40, Pages 5727-5731Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2008.07.079
Keywords
tetrahydropyrans; diastereoselectivity; aldehydes; allyltrimethylsilane; Bi(OTf)(3)center dot 4H(2)O; Sakurai-Prins-Ritter
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Funding
- CSIR, New Delhi
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The synthesis of 4-amidotetrahydropyrans has been achieved by a single-step Sakurai-Prins-Ritter reaction sequence in a domino fashion by the reaction of an aldehyde and allyltrimethylsilane in acetonitrile using Bi(OTf)(3) as catalyst. The present synthesis is highly efficient and diastereoselective. (C) 2008 Elsevier Ltd. All rights reserved.
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