Journal
TETRAHEDRON LETTERS
Volume 49, Issue 27, Pages 4306-4309Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2008.04.121
Keywords
phenyl isocyanate; vinyl aziridine; N-heterocyclic carbene; nickel; imidazolidinone; oxazolidinone; tetrahydro-[1,3]diazepin-2-one
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Funding
- NIGMS NIH HHS [R01 GM076125-03, R01 GM076125] Funding Source: Medline
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Thermal coupling of vinyl aziridines and phenyl isocyanate was evaluated. Although oxazolidinone products were predominant, some reactions afforded a seven-membered ring heterocycle. When Ni/IMes was employed as a catalyst, a wider array of vinyl aziridines underwent coupling reactions. The Ni catalyzed reactions generally afforded vinyl imidazolidinones as major products. Published by Elsevier Ltd.
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