Journal
TETRAHEDRON LETTERS
Volume 49, Issue 25, Pages 3983-3986Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2008.04.104
Keywords
palladium-catalyzed alkenylation; intramolecular C-C bond formation; silyl enol ether; bicyclo[3.3.1]nonane; trialkylamine
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An exceptional intramolecular palladium-catalyzed alkenylation of silyl enol ether in the absence of a fluoride additive was developed, and this reaction led to the construction of bicyclo[3.3.1]nonane ring system in reasonable yield. In this type of reactions, trialkylamines were employed as additives instead of previously indispensable fluoride additives. (C) 2008 Elsevier Ltd. All rights reserved.
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