Journal
TETRAHEDRON LETTERS
Volume 49, Issue 28, Pages 4402-4404Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2008.05.012
Keywords
hypervalent iodine; gamma-lactone; potassium monomethyl malonate; enolisable ketone
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A novel one-pot procedure for the synthesis of 3-carbomethoxy-4-aryl furan-2-(5H)-ones is reported via alpha-tosyloxylation of enolisable ketones with [hydroxy(tosyloxy)iodo]benzene, followed by treatment with potassium monomethyl malonate and K2CO3. (C) 2008 Elsevier Ltd. All rights reserved.
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