Journal
TETRAHEDRON
Volume 70, Issue 35, Pages 5619-5625Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2014.06.079
Keywords
Conjugate hydrocyanation; Dienone; Green chemistry; Potassium hexacyanoferrate(II); Regioselectivity
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Funding
- National Natural Science Foundation of China [21162024, 21362034]
- Key Laboratory of Eco-Environment-Related Polymer Materials for Ministry of Education
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A highly regioselective 1,4-conjugate hydrocyanation of dienones using potassium hexacyanoferrate(II) as an original eco-friendly cyanide source, benzoyl chloride as a promoter and potassium carbonate as a catalyst is described. This protocol has advantages of non-toxic cyanating agent, high regioselectivity, high yield, and simple work-up procedure. (C) 2014 Elsevier Ltd. All rights reserved.
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