Journal
TETRAHEDRON
Volume 70, Issue 23, Pages 3683-3690Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2014.04.017
Keywords
Ruthenium; Oxidation; Amide; Alcohol
Categories
Funding
- GSK
- Engineering and Physical Sciences Research Council
- NMR
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A wider investigation into the synthesis of secondary amides from primary alcohols using a hydrogen acceptor using commercially available [Ru(p-cymene)Cl-2](2) with bis(diphenylphosphino)butane (dppb) as the catalyst. The report looks at over 50 examples with varying functionality and steric bulk, whilst also covering the first reported results using microwave heating to effect the transformation. (C) 2014 Elsevier Ltd. All rights reserved.
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