Journal
TETRAHEDRON
Volume 70, Issue 38, Pages 6757-6762Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2014.07.068
Keywords
Acid-washed molecular sieves; Glycosylation; Promoter system; Thioglycosides
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Funding
- National Health Research Institutes
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The development of an alternative promoter system for thioglycoside activation comprising N-iodosuccinimide (NIS) and acid-washed molecular sieves (AW-300 MS) has been studied and found to mediate high-yielding coupling with a variety of glycosyl acceptors. The utility of this combination is further exemplified by its application to reactivity-based coupling of thioglycosides and sequential one-pot regioselective glycosylation. (C) 2014 Elsevier Ltd. All rights reserved.
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