Journal
TETRAHEDRON
Volume 70, Issue 14, Pages 2359-2369Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2014.02.039
Keywords
Methyl ketones; 1,3-Dicarbonyl compounds; Enaminones; Polysubstituted benzene derivatives; Cyclocondensations; Microwave assisted reactions
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Funding
- Slovenian Research Agency [P0-0502-0103, P1-0179, J1-6689-0103-04]
- Krka d.d. (Novo mesto, Slovenia)
- Lek d.d., a Sandoz Company (Ljubljana, Slovenia)
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Herein a simple one-pot metal-free synthesis of alkyl-, aryl-, heteroaryl- and alkoxycarbonyl substituted 1,3-bis(dimethylamino)benzene derivatives is described. The products were prepared from the corresponding methyl ketones or compounds with an a-methylene group in regard to the carbonyl group, using N,N-dimethylacetamide dimethyl acetal (DMADMA) as the reagent. (C) 2014 Published by Elsevier Ltd.
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