Journal
TETRAHEDRON
Volume 68, Issue 27-28, Pages 5356-5362Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2012.04.115
Keywords
Type I Ferrier Rearrangement; Iron(III) triflate; Tri-O-acetyl-D-glucal; 2,3-Unsaturated-O-glycoside
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Funding
- The Key Laboratory of Synthetic Chemistry of Natural Substances, Shanghai Institute of Organic Chemistry, CAS
- The Fundamental Research Funds for the Central Universities [11D10508]
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By using iron(III) triflate as catalyst, an improved method for the synthesis of 2,3-unsaturated-O-glycosides has been established. A series of 2,3-unsaturated-O-glucosides were obtained from 2,4,6-tri-O-acetyl-D-glucal in good yield and high anomeric selectivity. (c) 2012 Elsevier Ltd. All rights reserved.
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