Journal
TETRAHEDRON
Volume 67, Issue 5, Pages 866-871Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.12.040
Keywords
Microwave-assisted synthesis; DMF; Formamides; Dehalogenative amination; Purines
Categories
Funding
- Institute of Organic Chemistry and Biochemistry [OZ40550506]
- Ministry of Education, Youth and Sports of the Czech Republic, Centre for new antivirals and anti-neoplastics [1M0508]
- Youth and Sports of the Czech Republic
- Grant Agency of the Academy of Sciences of the Czech Republic [KJB400550903]
- Gilead Sciences and IOCB Research Centre
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The microwave-assisted decomposition of DMF was thoroughly studied and the reaction conditions (temperature, solvent effect, and effect of additives, such as acids, bases, and salts) were optimized for its use in amination reactions. The applicability of this expedient methodology in purine chemistry and with various formamides is demonstrated. (C) 2010 Elsevier Ltd. All rights reserved.
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