Journal
TETRAHEDRON
Volume 67, Issue 26, Pages 4753-4757Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.04.107
Keywords
Palladium-catalyzed; Reductive; Cyclization; Alkaloid; Salviadione
Categories
Funding
- National Science Foundation [CHE-0611096]
- NSF-EPSCoR [1002165R]
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An expedient synthesis of the alkaloid salviadione, the only to date isolated naturally occurring 1H-benzo [def]carbazole is described. The key step in the synthesis is a palladium-catalyzed, carbon monoxide-mediated reductive N-heterocyclization of a nitroarene with an adjacent alkene. (C) 2011 Elsevier Ltd. All rights reserved.
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