Journal
TETRAHEDRON
Volume 67, Issue 13, Pages 2462-2467Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.01.061
Keywords
Diethyl phosphite; N3-Substituted dihydropyrimidinones; N-Alkylation; P O cleavage
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Funding
- National Nature Science Foundation of China [20902073, 21062017]
- Natural Science Foundation of Gansu Province [096RJZA116]
- Northwest Normal University [nwnu-kjcxgc-03-64]
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N-Alkoxymethylation of heterocyclic compounds with diethyl phosphite via cleavage of P-O bond was investigated and a series of N3-ethoxymethylated heterocyclic compounds were synthesized. A mechanism in which diethyl phosphite acts as an efficient surrogate of ethanol was proposed and supported by several evidences. (C) 2011 Elsevier Ltd. All rights reserved.
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