Journal
TETRAHEDRON
Volume 67, Issue 8, Pages 1523-1529Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.01.001
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Funding
- Shanghai Municipal Committee of Science and Technology [08dj1400100-2]
- National Basic Research Program of China (973) [2009CB825300]
- National Natural Science Foundation of China [20472096, 20872162, 20672127, 20821002, 20732008]
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A new class of palladium(II) complexes of chelating NHC-N donor hybrid ligands, such as NHC-sulfonamide (6), NHC-phenoxyimine (11), NHC-phenylimine (14), and NHC-amine (15) have been successfully synthesized in modest yields from 1,1'-binaphthyl-2,2'-diamine (BINAM). These complexes have been characterized by all the spectroscopic data, and the structures of 6, 11, and 14 were also confirmed by single-crystal X-ray diffraction studies, exhibiting a tridentate chelating motif around the palladium center. (C) 2011 Elsevier Ltd. All rights reserved.
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