Journal
TETRAHEDRON
Volume 66, Issue 1, Pages 329-333Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.10.093
Keywords
Catalytic reduction; Chemoselectivity; Amines; Molybdenum; Silanes
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Funding
- Indian Institute of Science
- Ray Chemicals Pvt. Ltd
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A chemoselective, neutral, and efficient strategy for the reduction of azides to corresponding amines catalyzed by dioxobis(N,N,-diethyldithiocarbamato) molybdenum complex (1, MoO2[S2CNEt2](2)) in the presence of phenylsilane is discovered. This chemoselective reduction strategy tolerates a variety of reducible functional groups. (C) 2009 Elsevier Ltd. All rights reserved.
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